SYNTHESIS AND CHARACTERIZATION OF P- NITRO BENZYL BROMIDE FROM P- NITRO TOLUENE Authors: Patel DS , DAVE RH*, SANDHU SJ, GOHIL S, SOLANKI PD, THORIYA TA, RAM BM AND PATEL S
ABSTRACT
The raw material p- Nitro Toluene (PNT) was synthesized successfully using two different routes.
In the second route, we obtained p- Nitro Toluene (PNT) clear oily yellow-coloured liquid with a
boiling point of 2300C, yield of 54.67% and was confirmed by TLC analysis. This was then used
for the production of p- p-nitro benzyl Bromide (PNBBr) in one of the batches placed. The final
product p- Nitro Benzyl Bromide (PNBBr) was also successfully synthesized in 3 batches kept as
pale yellow to white coloured solid crystalline powder with a melting point ranging from 90-970C
of crude, washed, crystallized and recrystallized product. The yield obtained was also in sufficient
quantity of about 75%.
Keywords: p- Nitro Toluene, p- Nitro Benzyl Bromide, Nitration, Halogenation Publication date: 01/03/2026 https://ijbpas.com/pdf/2026/March/MS_IJBPAS_2026_9950.pdfDownload PDFhttps://doi.org/10.31032/IJBPAS/2026/15.3.9950